碳分子筛是七十年代出现的新型气相色谱固定相,它具有耐高温、耐腐蚀、柱效率高,柱寿命长,操作简便和重现性好等优点。从1973年以来,我们一直对此进行了研究,取得了良好的结果。现将几种碳分子筛在金属中气体分析上应用的结果介绍如下。
一、仪器和试剂 仪器:gc-790型金属中气体分析仪; 色谱分析条件:载气为氩气,氩气流量为20ml/min。
名称:填充柱
规格:3m*1/8
型号:TDX-01
应用:H2,空气,CO,CH4,及CO2的测定
Carbon molecular sieve is a new type of gas chromatography stationary phase that appeared in the 1970s. It has the advantages of high temperature resistance, corrosion resistance, high column efficiency, long column life, simple operation and good reproducibility. Since 1973, we have been conducting research on this and achieved good results. The results of the application of several carbon molecular sieves in gas analysis in metals are introduced as follows.
1. Apparatus and reagents Apparatus: gc-790 metal gas analyzer; chromatographic analysis conditions: the carrier gas is argon, and the argon flow rate is 20ml/min.
Name: Packed column
Specification: 3m*1/8
Model: TDX-01
Application: Determination of H2, Air, CO, CH4, and CO2